Calcination Quotes (4 quotes)
About eight days ago I discovered that sulfur in burning, far from losing weight, on the contrary, gains it; it is the same with phosphorus; this increase of weight arises from a prodigious quantity of air that is fixed during combustion and combines with the vapors. This discovery, which I have established by experiments, that I regard as decisive, has led me to think that what is observed in the combustion of sulfur and phosphorus may well take place in the case of all substances that gain in weight by combustion and calcination; and I am persuaded that the increase in weight of metallic calxes is due to the same cause... This discovery seems to me one of the most interesting that has been made since Stahl and since it is difficult not to disclose something inadvertently in conversation with friends that could lead to the truth I have thought it necessary to make the present deposit to the Secretary of the Academy to await the time I make my experiments public.
I prefer the spagyric chemical physicians, for they do not consort with loafers or go about gorgeous in satins, silks and velvets, gold rings on their fingers, silver daggers hanging at their sides and white gloves on their hands, but they tend their work at the fire patiently day and night. They do not go promenading, but seek their recreation in the laboratory, wear plain learthern dress and aprons of hide upon which to wipe their hands, thrust their fingers amongst the coals, into dirt and rubbish and not into golden rings. They are sooty and dirty like the smiths and charcoal burners, and hence make little show, make not many words and gossip with their patients, do not highly praise their own remedies, for they well know that the work must praise the master, not the master praise his work. They well know that words and chatter do not help the sick nor cure them... Therefore they let such things alone and busy themselves with working with their fires and learning the steps of alchemy. These are distillation, solution, putrefaction, extraction, calcination, reverberation, sublimination, fixation, separation, reduction, coagulation, tinction, etc.
In my youth I often asked what could be the use and necessity of smelting by putting powdered charcoal at the bottom of the furnace. Nobody could give me any other reason except that the metal and especially lead, could bury itself in the charcoal and so be protected against the action of the bellows which would calcine or dissipate it. Nevertheless it is evident that this does not answer the question. I accordingly examined the operation of a metallurgical furnace and how it was used. In assaying some litharge [lead oxide], I noticed each time a little charcoal fell into the crucible, I always obtained a bit of lead I do not think up to the present time foundry-men ever surmised that in the operation of founding with charcoal there was something [phlogiston] which became corporeally united with the metal.
The condensed air becomes attached to [the metallic calx], and adheres little by little to the smallest of its particles: thus its weight increases from the beginning to the end: but when all is saturated, it can take up no more.
— Jean Rey